There are three principal techniques used to measure carbon 14 content of any given sample— gas proportional counting, liquid scintillation counting, and accelerator mass spectrometry.
Gas proportional counting is a conventional radiometric dating technique that counts the beta particles emitted by a given sample. In this method, the carbon sample is first converted to carbon dioxide gas before measurement in gas proportional counters takes place.
No other scientific method has managed to revolutionize man’s understanding not only of his present but also of events that already happened thousands of years ago.
Archaeology and other human sciences use radiocarbon dating to prove or disprove theories.
Over the years, other secondary radiocarbon standards have been made.
Radiocarbon activity of materials in the background is also determined to remove its contribution from results obtained during a sample analysis.
When the stocks of Oxalic Acid I were almost fully consumed, another standard was made from a crop of 1977 French beet molasses.
The new standard, Oxalic Acid II, was proven to have only a slight difference with Oxalic Acid I in terms of radiocarbon content.
He is credited to be the first scientist to suggest that the unstable carbon isotope called radiocarbon or carbon 14 might exist in living matter. Libby and his team of scientists were able to publish a paper summarizing the first detection of radiocarbon in an organic sample. Libby who first measured radiocarbon’s rate of decay and established 5568 years ± 30 years as the half-life. Libby was awarded the Nobel Prize in Chemistry in recognition of his efforts to develop radiocarbon dating.1.
Standard errors are also reported in a radiocarbon dating result, hence the “±” values.
These values have been derived through statistical means.
A radiocarbon measurement is termed a conventional radiocarbon age (CRA).
The CRA conventions include (a) usage of the Libby half-life, (b) usage of Oxalic Acid I or II or any appropriate secondary standard as the modern radiocarbon standard, (c) correction for sample isotopic fractionation to a normalized or base value of -25.0 per mille relative to the ratio of carbon 12/carbon 13 in the carbonate standard VPDB – Cretaceous belemnite formation at Peedee in South Carolina, (d) zero BP (Before Present) is defined as AD 1950, and (e) the assumption that global radiocarbon levels are constant.